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單壁納米碳管的純化研究
A purification method to remove the metal catalysts and impurity carbon materials from arc-discharge-grownsingle-walled carbon nanotubes (SWCNTs) has been developed. Microporous membrane and the oxidation in the airfor the crude SWCNTs were used to eliminate the coexisting metal catalysts nanoparticles, carbon nanoparticles andamorphous carbon. Then we used the high resolution transmission electron microscopy (HRTEM) to characterizethe crude SWCNTs prepared by arc-discharge method and the purified SWCNTs. The Raman spectra and thethermogravimetric analysis (TGA) were also utilized to analyze the approach of our purification for SWCNTs. Withthis method the SWCNTs with the purity more than 95% could be obtained.
作 者: 王新慶 王淼 李振華 朱海濱 王鳳飛 盧煥明 何丕模 作者單位: 王新慶,王淼(浙江大學(xué)物理系,杭州,310027;浙江大學(xué)微系統(tǒng)研究與開(kāi)發(fā)中心,杭州,310027)李振華(浙江大學(xué)力學(xué)系,杭州,310027)
朱海濱,王鳳飛,何丕模(浙江大學(xué)物理系,杭州,310027)
盧煥明(浙江大學(xué)硅材料國(guó)家重點(diǎn)實(shí)驗(yàn)室,杭州,310027)
刊 名: 無(wú)機(jī)化學(xué)學(xué)報(bào) ISTIC SCI PKU 英文刊名: CHINESE JOURNAL OF INORGANIC CHEMISTRY 年,卷(期): 2003 19(6) 分類(lèi)號(hào): O6130.71 關(guān)鍵詞: 單壁納米碳管 拉曼光譜 熱重分析 single-walled carbon nanotube(SWCNTs) Raman spectra thermogravimetric analysis (TGA)【單壁納米碳管的純化研究】相關(guān)文章:
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